St 396 Set 4 chromite (UC # 523-9) TakeOff = 52.5 KiloVolts = 15 Beam Current = 20 Beam Size = 2 Number of Lines: 6 Number of 'Good' Lines: 6
Elemental Wt. % Total: 100.509 Average Total Oxygen: 33.111 Average Calcu. Oxygen: 32.034 Average Excess Oxygen: 1.077 Average Atomic Weight: 27.814 Average Atomic Number: 17.543 Average ZAF Iteration: 4.00 Average MAN Iteration: 3.00 Oxygen Calculated by Cation Stoichiometry and Included in the Matrix Correction
Results in Elemental Weight Percents
SPEC: O Ca Mn Ti Ni V TYPE: CALC SPEC SPEC SPEC SPEC SPEC
AVER: 33.111 .000 .225 .300 .000 .122 SDEV: .089 .000 .000 .000 .000 .000
ELEM: Si Fe Al Mg Cr BGDS: MAN MAN MAN MAN MAN ABS%: -27.72 -1.87 -35.01 -44.69 .06 TIME: 10.00 10.00 10.00 10.00 10.00
ELEM: Si Fe Al Mg Cr SUM 301 .006 20.690 7.819 6.236 32.066 100.660 302 .000 20.762 7.673 6.312 31.778 100.168 303 .000 20.777 7.821 6.153 32.062 100.620 304 .000 20.894 7.647 6.408 31.751 100.409 305 .000 20.865 7.662 6.349 32.145 100.877 306 .007 20.780 7.705 6.213 31.925 100.319
AVER: .002 20.795 7.721 6.278 31.955 100.509 SDEV: .003 .074 .079 .094 .164 SERR: .001 .030 .032 .039 .067 %RSD: 156.6 .4 1.0 1.5 .5
PUBL: .005 20.692 7.690 6.290 31.905 100.271 %VAR: -56.86 .50 .40 -.18 .16 STDS: 14 395 13 12 24
STKF: .4176 .6775 .4474 .4920 .6402 STCT: 2681.1 10798.7 8895.2 6366.5 9872.9
UNKF: .0000 .1853 .0512 .0367 .3061 UNCT: -.1 2953.8 1017.4 474.6 4719.6 UNBG: 3.0 51.3 10.9 2.3 32.4
ZCOR: 1.3202 1.1221 1.5089 1.7119 1.0441 KRAW: .0000 .2735 .1144 .0745 .4780 PKBG: .97 58.53 94.55 206.31 146.49
Results in Oxide Weight Percents
SPEC: O CaO MnO TiO2 NiO V2O3 TYPE: CALC SPEC SPEC SPEC SPEC SPEC
AVER: 1.077 .000 .291 .500 .000 .179 SDEV: .000 .000 .000 .000 .000 .000
ELEM: SiO2 FeO Al2O3 MgO Cr2O3 SUM 301 .012 26.617 14.774 10.342 46.867 100.660 302 .000 26.710 14.498 10.467 46.445 100.168 303 .000 26.730 14.778 10.203 46.861 100.620 304 .000 26.880 14.448 10.626 46.407 100.409 305 .000 26.842 14.476 10.528 46.983 100.877 306 .016 26.733 14.558 10.303 46.661 100.319
AVER: .005 26.752 14.589 10.412 46.704 100.509 SDEV: .007 .095 .150 .157 .239 SERR: .003 .039 .061 .064 .098 %RSD: 156.6 .4 1.0 1.5 .5
Results in Atomic Percents
SPEC: O Ca Mn Ti Ni V TYPE: CALC SPEC SPEC SPEC SPEC SPEC
AVER: 57.267 .000 .113 .173 .000 .066 SDEV: .028 .000 .000 .000 .000 .000
ELEM: Si Fe Al Mg Cr SUM 301 .006 10.230 8.002 7.086 17.030 100.000 302 .000 10.321 7.895 7.210 16.967 100.000 303 .000 10.286 8.014 6.999 17.048 100.000 304 .000 10.361 7.848 7.301 16.911 100.000 305 .000 10.305 7.832 7.205 17.053 100.000 306 .007 10.320 7.920 7.090 17.030 100.000
AVER: .002 10.304 7.919 7.149 17.007 100.000 SDEV: .003 .044 .076 .109 .056 SERR: .001 .018 .031 .045 .023 %RSD: 156.7 .4 1.0 1.5 .3
Detection limit at 99 % Confidence in Elemental Weight Percent (Single Line):
ELEM: Si Fe Al Mg Cr 301 .034 --- --- --- --- 302 .034 --- --- --- --- 303 .034 --- --- --- --- 304 .034 --- --- --- --- 305 .034 --- --- --- --- 306 .034 --- --- --- ---
AVER: .034 --- --- --- --- SDEV: .000 --- --- --- --- SERR: .000 --- --- --- ---
Percent Analytical Error (Single Line):
ELEM: Si Fe Al Mg Cr 301 288.4 .6 1.0 1.5 .5 302 -116.0 .6 1.0 1.5 .5 303 -1941.0 .6 1.0 1.5 .5 304 -316.6 .6 1.0 1.4 .5 305 -311.6 .6 1.0 1.5 .5 306 227.1 .6 1.0 1.5 .5
AVER: -361.6 .6 1.0 1.5 .5 SDEV: 815.9 .0 .0 .0 .0 SERR: 333.1 .0 .0 .0 .0
Range of Homogeneity in +/- Elemental Weight Percent (Average of Sample):
ELEM: Si Fe Al Mg Cr 60ci .000 .028 .031 .035 .059 80ci .000 .045 .050 .057 .095 90ci .000 .061 .069 .077 .130 95ci .000 .078 .088 .099 .166 99ci .000 .122 .138 .155 .260
Test of Homogeneity at 1.0 % Precision (Average of Sample):
ELEM: Si Fe Al Mg Cr 60ci no yes yes yes yes 80ci no yes yes yes yes 90ci no yes yes no yes 95ci no yes no no yes 99ci no yes no no yes
Level of Homogeneity in +/- Percent (Average of Sample):
ELEM: Si Fe Al Mg Cr 60ci 4.7 .1 .4 .6 .2 80ci 7.5 .2 .7 .9 .3 90ci 10.3 .3 .9 1.2 .4 95ci 13.1 .4 1.1 1.6 .5 99ci 20.6 .6 1.8 2.5 .8
Detection Limit in Elemental Weight Percent (Average of Sample):
ELEM: Si Fe Al Mg Cr 60ci .003 --- --- --- --- 80ci .005 --- --- --- --- 90ci .007 --- --- --- --- 95ci .010 --- --- --- --- 99ci .015 --- --- --- ---
Analytical Sensitivity in Elemental Weight Percent (Average of Sample):
ELEM: Si Fe Al Mg Cr 60ci .000 .039 .044 .050 .084 80ci .000 .063 .071 .080 .134 90ci .000 .086 .097 .110 .184 95ci .000 .110 .124 .140 .234 99ci .001 .172 .195 .219 .367
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